Volume 100 (2023)
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Discussion Addendum for: Indium-Catalyzed Heteroaryl-Heteroaryl Bond Formation through Nucleophilic Aromatic Substitution: Preparation of 2-Methyl-3-(thien-2-yl)-1H-indole
Teruhisa Tsuchimoto
Org. Synth. 2023, 100, 287
DOI: 10.15227/orgsyn.100.0287
Original Article: Org. Synth. 2014, 91, 273

Reaction scheme
Visible-light-mediated Oxidative Debenzylation of 3-O-Benzyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose
Amiera Madani, Eric T. Sletten, Cristian Cavedon, Peter H. Seeberger, and Bartholomäus Pieber
Org. Synth. 2023, 100, 271
DOI: 10.15227/orgsyn.100.0271
Checked by: Kevin Lee and Dirk Trauner

Reaction scheme
Synthesis of 2-Phenyl-4,6-bis(trifluoromethyl)pyridine via NH4I/Na2S2O4-Mediated Cyclization of Ketoxime Acetates
Huawen Huang, Zhenhua Xu, and Guo-Jun Deng
Org. Synth. 2023, 100, 248
DOI: 10.15227/orgsyn.100.0248
Checked by: Hisahiro Morozumi, Koichi Hagiwara, and Masayuki Inoue

Reaction scheme
Visible-Light-Promoted C-S Cross-Coupling Reaction for Synthesis of Aromatic Thioethers
Yingjun Lan, Junhua Xu, Chern-Hooi Lim, Garret M. Miyake, and Bin Liu
Org. Synth. 2023, 100, 234
DOI: 10.15227/orgsyn.100.0234
Checked by: Luca McDermott, Zachary Walters, and Neil K. Garg

Reaction scheme
Synthesis of Potassium 5-Bromopentyltrifluoroborate via Hydroboration of a Haloalkene
Sarah J. Burke, Latifah M. Alhthlol, James M. Gamrat, Giulia Mancini, Christopher L. Orme, Jacqueline R. Santhouse, Dylan T. Tomares, and John W. Tomsho
Org. Synth. 2023, 100, 218
DOI: 10.15227/orgsyn.100.0218
Checked by: Philip Boehm and Sarah E. Reisman

Reaction scheme
Synthesis of Phenols from Benzoic Acids
Wenzhang Xiong, Rui Wang, Zhengqiang Liu, Feng Peng, Ralph Zhao, and Wenbo H. Liu
Org. Synth. 2023, 100, 199
DOI: 10.15227/orgsyn.100.0199
Checked by: Martina Drescher, Saad Shaaban and Nuno Maulide

Reaction scheme
Synthesis of Enantioenriched NH-Sulfoximines by NH Transfer to Sulfoxides Using Ammonium Carbamate and (Diacetoxyiodo)benzene
Edward L. Briggs, Tsz-Kan Ma, Zhenhao Zhong, Arianna Tota, Leonardo Degennaro, Renzo Luisi and James A. Bull
Org. Synth. 2023, 100, 186
DOI: 10.15227/orgsyn.100.0186
Checked by: Ellie Plachinski and Tehshik Yoon

Reaction scheme
Synthesis of a 2,5-Bis(tert-butyldimethylsilyloxy)furan and its Reaction with Benzyne
Jessica E. Budwitz and Christopher G. Newton
Org. Synth. 2023, 100, 159
DOI: 10.15227/orgsyn.100.0159
Checked by: Dave J. Charboneau, Jordan K. Thompson, and Sarah E. Reisman

Reaction scheme
α-Oxamination of Amides via Electrophilic Activation
Miran Lemmerer, Ján Matyašovský, Roberto Tinelli and Nuno Maulide
Org. Synth. 2023, 100, 136
DOI: 10.15227/orgsyn.100.0136
Checked by: Colin Knus, Jaime Martín, Jorge A. González, and Cristina Nevado

Reaction scheme
Kathleen J. Berger, Balu D. Dherange, Megan Morales, Julia L. Driscoll, A. Kaan Tarhan, and Mark D. Levin
Org. Synth. 2023, 100, 113
DOI: 10.15227/orgsyn.100.0113
Checked by: Yinuo Zheng and Pauline Chiu

Reaction scheme
α-Arylation of Cyclopentanones by Palladium/Enamine Cooperative Catalysis
Yibin Xue, Arjuna Parsad, and Guangbin Dong
Org. Synth. 2023, 100, 99
DOI: 10.15227/orgsyn.100.0099
Checked by: Jaejoong Han, Masanori Nagatomo, and Masayuki Inoue

Reaction scheme
Synthesis of Diethyl (1-Diazo-2-oxopropyl)phosphonate
Cholapat Varongchayakul and Rick L. Danheiser
Org. Synth. 2023, 100, 84
DOI: 10.15227/orgsyn.100.0084
Checked by: Michael D. Clift, Steve M. Richter, Zhe Wang, and Seble Wagaw

Reaction scheme
Preparation of N-Boc-3-methylpyrrole via Anionic Rearrangement
Daniel P. Graeff, Noah J. Sims, Quentin R. Savage, Richard K. Jackson, III, Amy C. Jackson, Danielle M. Lawson, Madelyn R. Wixom, and John L. Wood
Org. Synth. 2023, 100, 61
DOI: 10.15227/orgsyn.100.0061
Checked by: Yuya Shiga, Haruka Fujino, and Masayuki Inoue

Reaction scheme
Synthesis of NH-Sulfoximines from Sulfides Using Ammonium Carbamate and (Diacetoxyiodo)benzene to Transfer NH and O
Arianna Tota, Mauro Spennacchio, Edward L. Briggs, Tsz-Kan Ma, Zhenhao Zhong, Leonardo Degennaro, James A. Bull and Renzo Luisi
Org. Synth. 2023, 100, 48
DOI: 10.15227/orgsyn.100.0048
Checked by: Ellie Plachinski and Tehshik Yoon

Reaction scheme
Discussion Addendum for: Rh(I)-Catalyzed Allenic Pauson-Khand Reaction
Eric D. Deihl, Fatemeh Haghighi, and Kay M. Brummond
Org. Synth. 2023, 100, 29
DOI: 10.15227/orgsyn.100.0029
Original Article: Org. Synth. 2017, 94, 123

Reaction scheme
Preparation of Highly-Substituted Pyridines via Diels-Alder Reactions of Vinylallenes and Tosyl Cyanide
Nathan H. Faialaga, Christian Gomez, Samuel G. Bartko, Philipp Natho, and Rick L. Danheiser
Org. Synth. 2023, 100, 4
DOI: 10.15227/orgsyn.100.0004
Checked by: Christopher C. Nawrat and Kevin R. Campos

Reaction scheme
Introducing Volume 100 of Organic Syntheses
Rick L. Danheiser
Org. Synth. 2023, 100, 1
DOI: 10.15227/orgsyn.100.0001

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors