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1
Preparation of tBu-MsFluind-Br
Lucas Wagner and Josep Cornella
Org. Synth. 2025, 102,
350
DOI: 10.15227/orgsyn.102.0350
Checked by: Szymon Maciej Kosc, Katherine Clark, and Darren Dixon
2
Synthesis of 6-Methoxy-2-methyl-2-(4-methylpent-3-en-1-yl)chroman-4-one via Kabbe Condensation
Stephen A. Chamness, Emily F. Traficante, Trenton R. Vogel, and Corinna S. Schindler
Org. Synth. 2025, 102,
335
DOI: 10.15227/orgsyn.102.0335
Checked by: Max Neumann and Tehshik Yoon
3
Synthesis of gem-Difluoroalkenes through Ramberg-Bäcklund Reaction of Alkyltriflones
Motoo Ohtsuka, Yasuyo Tahara-Tezuka, Yuuki Maekawa, Cathleen M. Crudden, and Masakazu Nambo
Org. Synth. 2025, 102,
315
DOI: 10.15227/orgsyn.102.0315
Checked by: Nikolaos Skoulikas, Lorenz Erlbacher and Nuno Maulide
4
OS Techniques
Glass Cannula for Bulb-to-Bulb Cold Transfer
Kaylin N. Flesch, Tyler J. Fulton, Nathan Hart, and Brian M. Stoltz
Org. Synth. 2025, 102,
303
DOI: 10.15227/orgsyn.102.0303
Checked by: Mira Milic and Christopher D. Vanderwal
5
OS Techniques
Purification of Organic Compounds by Flash Column Chromatography
Benjamin D. Senzer, Cholapat Varongchayakul, Rick L. Danheiser*, Brian Daniels, and Vy M. Dong*
Org. Synth. 2025, 102,
276
DOI: 10.15227/orgsyn.102.0276
Checked by: Katerina Scotchburn and Sophie A. L. Rousseaux
6
Editorial
Announcing "OS Techniques" - A New Category of Articles in Organic Syntheses
Rick L. Danheiser
Org. Synth. 2025, 102,
273
DOI: 10.15227/orgsyn.102.0273
7
Rapid Access to Enantiopure Protected (R)-Paraconyl Alcohol
Haylie E. Hennigan, Namuunzul Otgontseren, and Elizabeth I. Parkinson
Org. Synth. 2025, 102,
251
DOI: 10.15227/orgsyn.102.0251
Checked by: David A. Petrone and Kevin R. Campos
8
Efficient Preparation of Chiral Hydroxylamines via Nickel-Catalyzed Asymmetric Hydrogenation of Oximes
Bowen Li, Jianzhong Chen, and Wanbin Zhang
Org. Synth. 2025, 102,
236
DOI: 10.15227/orgsyn.102.0236
Checked by: Greg Storer and Nathan Ide
9
Large-Scale Syntheses of Silanoxy-Tetrahydrofurans via Stereospecific [5,5]-Rearrangements of Silanol Epoxides
Silver Raju and Shyam Sathyamoorthi
Org. Synth. 2025, 102,
217
DOI: 10.15227/orgsyn.102.0217
Checked by: Nnamdi Akporji and Kevin Campos
10
Iodine-Catalyzed Stereospecific anti-Diamination of trans-?-Methylstyrene
Takeshi Sugiyama, Chiyuki Naito, and Satoshi Minakata
Org. Synth. 2025, 102,
203
DOI: 10.15227/orgsyn.102.0203
Checked by: Shun Kawano, Juri Sakata, and Hidetoshi Tokuyama
11
Synthesis of 1-(phenylsulfonyl)bicyclo[1.1.0]butane from Methyl Phenyl Sulfone and Epichlorohydrin
Joanna E. Muir, Myunggi Jung, and Vincent N. G. Lindsay
Org. Synth. 2025, 102,
185
DOI: 10.15227/orgsyn.102.0185
Checked by: Yu-Che Chang and M. Kevin Brown
12
Synthesis of Serine Derived Oxazolines Using a Molybdenum Dioxide Catalyst
Wyatt C. Powell, Garrett E. Evenson, and Maciej A. Walczak
Org. Synth. 2025, 102,
156
DOI: 10.15227/orgsyn.102.0156
Checked by: Zengsheng Yin and Pauline Chiu
13
Preparation of (Z)-N-Phenoxybenzimidoyl Chloride
Joseph P. Lokant, Ross M. Dare, and David A. Nagib
Org. Synth. 2025, 102,
143
DOI: 10.15227/orgsyn.102.0143
Checked by: Souvik Adak and M. Kevin Brown
14
C(sp2)-S Cross-Coupling Reactions with Adaptive Dynamic Homogeneous Catalysis: Synthesis of Ethyl 4-((3-Ethoxy-3-oxopropyl)thio)benzoate
Florence Babawale, Indrajit Ghosh, Burkhard König
Org. Synth. 2025, 102,
128
DOI: 10.15227/orgsyn.102.0128
Checked by: Nicholas D. D'Arcy-Evans, Evan Rutter, and Darren J. Dixon
15
Photoexcited Nitroarenes for the Anaerobic Cleavage of Alkenes
Lifeng Yin, Ben S. Kozloff, Ning Deng, Preya D. Persaud, Ajay H. Bansode, Dan E. Wise, Jenny S. Martinez, and Marvin Parasram
Org. Synth. 2025, 102,
114
DOI: 10.15227/orgsyn.102.0114
Checked by: Cailean Bonella, Alberto Ristache, and Darren Dixon
16
Large-Scale NaBr/Selectfluor Mediated Alcohol Oxidation: Conversion of (-)-Borneol into (-)-Camphor
Shyam Sathyamoorthi
Org. Synth. 2025, 102,
100
DOI: 10.15227/orgsyn.102.0100
Checked by: Sergio Armentia Matheu, Saad Shaaban, and Nuno Maulide
17
Copper-Catalyzed Suzuki-Miyaura Coupling of Unactivated Alkyl Halides with Arylborons
Yonglei Zhou, Jian Li, and Weilong Xie
Org. Synth. 2025, 102,
86
DOI: 10.15227/orgsyn.102.0086
Checked by: Kathryn M. Weber and Tehshik P. Yoon
18
A General Method for C-Alkylation of Nitroalkanes with Alkyl Halides: Nickel Photoredox Dual-Catalyzed C-Alkylation of Nitroalkanes
Sina Rezazadeh, Allyssa M. Conner, and Donald A. Watson
Org. Synth. 2025, 102,
64
DOI: 10.15227/orgsyn.102.0064
Checked by: Neetu Sharma and M. Kevin Brown
19
Preparation of 1,3-Dihydroxyphenazine
Trevor Dzwiniel, Emma Markun, James A. Kaduk, Aaron Hollas, Krzystof Pupek, and Nicholas Boaz
Org. Synth. 2025, 102,
45
DOI: 10.15227/orgsyn.102.0045
Checked by: Uros Vezonik, Florian Doubek and Nuno Maulide
20
Synthesis of Borane-Ammonia and its Application in the Titanium Tetrachloride Catalyzed Reduction of Carboxylic Acids, Including N-Protected Amino Acids
Henry J. Hamann, Abdulkhaliq A. Alawaed, and P. Veeraraghavan Ramachandran
Org. Synth. 2025, 102,
19
DOI: 10.15227/orgsyn.102.0019
Checked by: Gwyndaf A. Oliver, Konstantin Gunther and Nuno Maulide
21
Sharpless Epoxidation of Divinyl Carbinol
Klaus-Peter Ruhmann, Paula Mora, and Dirk Trauner
Org. Synth. 2025, 102,
1
DOI: 10.15227/orgsyn.102.0001
Checked by: Aaron L. Featherston, Nathan Ide, and Seble Wagaw
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