Volume 101 (2024)
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Preparation of 2-Chloro-1-(1-ethoxyvinyl)pyridinium Triflate
John P. Frank, William R. Strutton, Joel K. A. Adade, and Max M. Majireck
Org. Synth. 2024, 101, 242
DOI: 10.15227/orgsyn.101.0242
Checked by: Christopher C. Nawrat and Kevin Campos

Reaction scheme
Platinum-Catalyzed Enantioselective Diboration of Monosubstituted Alkenes
Chenpeng Gao, Paul S. Lee, and James P. Morken
Org. Synth. 2024, 101, 229
DOI: 10.15227/orgsyn.101.0229
Checked by: Matthieu Maciejewski and Tehshik Yoon

Reaction scheme
Chromatography-Free and Chlorinated Solvent-Free Preparation of 2,5-dibromohexanediamide (DBHDA)
Ben Bower, Sébastien R. G. Galan, and Benjamin G. Davis
Org. Synth. 2024, 101, 207
DOI: 10.15227/orgsyn.101.0207
Checked by: Ruby Long Ying Chan and Pauline Chiu

Reaction scheme
Intramolecular Coupling for General Synthesis of Backbone Substituted Bicyclo[1.1.1]pentyl Boronates
Jet Tsien, Yangyang Yang, René García-Del Valle, Jonathan M. E. Hughes, Byron K. Peters, Rohan R. Merchant, and Tian Qin
Org. Synth. 2024, 101, 181
DOI: 10.15227/orgsyn.101.0181
Checked by: Sota Akiyama, Paul Sinclair and Richmond Sarpong

Reaction scheme
Difluoromethylation of Phenols
Allison T. Hands, Zachary G. Walters, Jacob P. Sorrentino, and Neil K. Garg
Org. Synth. 2024, 101, 164
DOI: 10.15227/orgsyn.101.0164
Checked by: Yi Xiao, Milos Vavrik and Nuno Maulide

Reaction scheme
Nickel-catalyzed Amination of Aryl Chlorides
Zachary G. Walters, Daniel W. Turner, and Neil K. Garg
Org. Synth. 2024, 101, 150
DOI: 10.15227/orgsyn.101.0150
Checked by: Prashansa B. Kannangara and M. Kevin Brown

Reaction scheme
Tandem Fragmentation/Olefination for Production of Neopentylene-Tethered 1,6-Enynes from Dimedone
Kh Tanvir Ahmed, A. C. Martin, Gabriella O. Wabler, Kristen S. Nerbecki, and Gregory B. Dudley
Org. Synth. 2024, 101, 124
DOI: 10.15227/orgsyn.101.0124
Checked by: Hyung Joo Kim and Tehshik Yoon

Reaction scheme
Synthesis of 5-(1-Diazo-2-ethoxy-2-oxoethyl) dibenzo[b,d]thiophenium Triflate
Brigitte Worbs, Sven Timmann, Feng Peng, Ralph Zhao, and Manuel Alcarazo
Org. Synth. 2024, 101, 109
DOI: 10.15227/orgsyn.101.0109
Checked by: Partha Sarathi Hazra and Kevin Brown

Reaction scheme
Discussion Addendum for: Mild Conversion of Tertiary Amides to Aldehydes Using Cp2Zr(H)Cl (Schwartz's Reagent)
Narsihmulu Cheryala, Rui Shi, Shelby Mcguire, Naresh Gantasala, Nagarjun Reddy Vantaddu, Ravikrishna Dada, Nan Wang, Shameem S. Syeda, Hira Khalid, and Gunda I. Georg
Org. Synth. 2024, 101, 81
DOI: 10.15227/orgsyn.101.0081
Original Article: Org. Synth. 2011, 88, 427

Reaction scheme
Preparation of Radical Clocks Bearing Carbonyl Groups: Synthesis of N-Methoxy-N-methylspiro[cyclopropane-1,9'-fluorene]-2-carboxamide
Nicole D. Bartolo, Ryan N. Robson, Collin H. Witt, and K. A. Woerpel
Org. Synth. 2024, 101, 61
DOI: 10.15227/orgsyn.101.0061
Checked by: Kevin Lee and Dirk Trauner

Reaction scheme
Cobalt-catalyzed Radical Olefin Isomerization: Retrocycloisomerization of (-)-Caryophyllene Oxide to (-)-Humulene Oxide II
Eleanor M. Landwehr and Ryan A. Shenvi
Org. Synth. 2024, 101, 51
DOI: 10.15227/orgsyn.101.0051
Checked by: Emily P. Chen and Sarah E. Reisman

Reaction scheme
Metal-Free Aziridination of Alkenes with Free Amines by Thianthrenation
Ming-Shang Liu and Wei Shu
Org. Synth. 2024, 101, 34
DOI: 10.15227/orgsyn.101.0034
Checked by: Michael D. Zott and Dirk Trauner

Reaction scheme
Synthesis of Deuterated 1H-Indole-3-carboxaldehyde via Catalytic Vilsmeier-Haack Reaction
Jing Xue, Yushan Zhang, Bing Zhong and Jin-Dong Yang
Org. Synth. 2024, 101, 21
DOI: 10.15227/orgsyn.101.0021
Checked by: Paolo Piacentini, Omar Abdo and Nuno Maulide

Reaction scheme
Synthesis of Secondary Benzylic Alcohols by Reductive Arylation of Aldehydes: α-Phenyl-6-quinolinemethanol
Gilian T. Thomas, Eric S. Isbrandt and Stephen G. Newman
Org. Synth. 2024, 101, 1
DOI: 10.15227/orgsyn.101.0001
Checked by: Christopher C. Nawrat and Kevin Campos

Reaction scheme

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All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors