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Volume 98 (2021)
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1
Mild mono-Acylation of 4,5-Diiodoimidazole: Preparation of 1-(5-Iodo-1H-imidazole-4-yl)pent-4-en-1-one
Michael Morgen, Jasmin Lohbeck, and Aubry K. Miller
Org. Synth. 2021, 98, 171
DOI: 10.15227/orgsyn.098.0171
Checked by: Anji Chen, Hari P. R. Mangunuru, Nathaniel D. Kaetzel, Gopal Sirasani, and Chris Senanayake

Reaction scheme
2
Synthesis of the Isocyanide Building Block Asmic, anisylsulfanylmethylisocyanide
Embarek Alwedi, Bilal Altundas, Allen Chao, Zachary L. Ziminsky, Maanasa Natrayan, and Fraser F. Fleming
Org. Synth. 2021, 98, 147
DOI: 10.15227/orgsyn.098.0147
Checked by: Anthony J. Fernandes, Martina Drescher, and Nuno Maulide

Reaction scheme
3
Palladium-Catalyzed Hydrodefluorination of Fluoroarenes
Joseph J. Gair, Ronald L. Grey, Simon Giroux, and Michael A. Brodney
Org. Synth. 2021, 98, 131
DOI: 10.15227/orgsyn.098.0131
Checked by: Vincent Porte, Daniel Kaiser, and Nuno Maulide

Reaction scheme
4
Discussion Addendum for: Preparation of (S)-tert-ButylPyOx and Palladium-Catalyzed Asymmetric Conjugate Addition of Arylboronic Acids
Stephen R. Sardini and Brian M. Stoltz
Org. Synth. 2021, 98, 117
DOI: 10.15227/orgsyn.098.0117
Original Article: Org. Synth. 2015, 92, 247

Reaction scheme
5
Synthesis of a Phosphorous Sulfur Incorporating Reagent for the Enantioselective Synthesis of Thiophosphates
Prantik Maity, Amitha S. Anandamurthy, Vijaykumar Shekarappa, Rajappa Vaidyanathan, Bin Zheng, Jason Zhu, Michael A Schmidt, Richard J. Fox, Kyle W. Knouse, Julien C. Vantourout, Phil S. Baran, and Martin D. Eastgate
Org. Synth. 2021, 98, 97
DOI: 10.15227/orgsyn.098.0097
Checked by: Álvaro Gutiérrez-Bonet and Kevin Campos

Reaction scheme
6
Cu-catalyzed Allylic Perfluoroalkylation of Alkenes Using Perfluoro Acid Anhydrides: Preparation of N-(5,5,5-Trifluoro-2-penten-1-yl)phthalimide
Yuma Aoki, Shintaro Kawamura, and Mikiko Sodeoka
Org. Synth. 2021, 98, 84
DOI: 10.15227/orgsyn.098.0084
Checked by: Martina Drescher, Daniel Kaiser, and Nuno Maulide

Reaction scheme
7
Palladium-Catalyzed Acetylation of Arylbromides
Milauni M. Mehta, Andrew V. Kelleghan, and Neil K. Garg
Org. Synth. 2021, 98, 68
DOI: 10.15227/orgsyn.098.0068
Checked by: Martina Drescher, Daniel Kaiser, Nuno Maulide, Zach Ariki, Yuki Maekawa, and Cathleen Crudden

Reaction scheme
8
Reductive Deuteration of Ketones with Magnesium and D2O for the Synthesis of α-Deutero-o-methyl-benzhydrol
Nengbo Zhu, Wen-Ming Wan, and Hongli Bao
Org. Synth. 2021, 98, 51
DOI: 10.15227/orgsyn.098.0051
Checked by: Yuuki Watanabe, Koichi Hagiwara, and Masayuki Inoue

Reaction scheme
9
Chiral Organoiodine-catalyzed Enantioselective Oxidative Dearomatization of Phenols
Muhammet Uyanik, Shinichi Ishizaki, and Kazuaki Ishihara
Org. Synth. 2021, 98, 28
DOI: 10.15227/orgsyn.098.0028
Checked by: Tao Wang and Kevin Campos

Reaction scheme
10
Synthesis of Chiral Organoiodine Catalyst for Enantioselective Oxidative Dearomatization Reactions: N,N'-(2S,2'S )-(2-Iodo-1,3-phenylene)bis(oxy)bis(propane-2,1-diyl)bis(2,4,6-trimethylbenzamide)
Muhammet Uyanik, Shinichi Ishizaki and Kazuaki Ishihara
Org. Synth. 2021, 98, 1
DOI: 10.15227/orgsyn.098.0001
Checked by: Cayetana Zarate and Kevin Campos

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors
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