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Volume 94 (2017)
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1
Preparation of Benzyl((R)-2-(4-(benzyloxy)phenyl)-2-((tert-butoxycarbonyl)amino)acetyl)-D-phenylalaninate using Umpolung Amide Synthesis
Matthew T. Knowe, Sergey V. Tsukanov, and Jeffrey N. Johnston
Org. Synth. 2017, 94, 388
DOI: 10.15227/orgsyn.094.0388
Checked by: Manuela Brütsch, Estíbaliz Merino, and Cristina Nevado

Reaction scheme
2
Synthesis of Methyl trans-Oxazolidine-5-carboxylate, a Chiral Synthon for threo-β-Amino-α-hydroxy Acid
Youngran Seo, Jae Won Yoo, Yoonjae Lee, Boram Lee, Bonghyun Kim, and Young Gyu Kim
Org. Synth. 2017, 94, 372
DOI: 10.15227/orgsyn.094.0372
Checked by: Zhaobin Han and Kuiling Ding

Reaction scheme
3
Synthesis of N-Boc-N-Hydroxymethyl-L-phenylalaninal
Jae Won Yoo, Youngran Seo, Dongwon Yoo, and Young Gyu Kim
Org. Synth. 2017, 94, 358
DOI: 10.15227/orgsyn.094.0358
Checked by: Zhaobin Han and Kuiling Ding

Reaction scheme
4
Preparation of N-Sulfinyl Aldimines using Pyrrolidine as Catalyst via Iminium Ion Activation
Sara Morales, Alfonso García Rubia, Eduardo Rodrigo, José Luis Aceña, José Luis García Ruano, and M. Belén Cid
Org. Synth. 2017, 94, 346
DOI: 10.15227/orgsyn.094.0346
Checked by: Gabrielle St-Pierre, Christopher J. Borths, and Margaret M. Faul

Reaction scheme
5
Water-promoted, Open-flask Synthesis of Amine-boranes: 2-Methylpyridine-borane (2-Picoline-borane)
Ameya S. Kulkarni and P. Veeraraghavan Ramachandran
Org. Synth. 2017, 94, 332
DOI: 10.15227/orgsyn.094.0332
Checked by: Hwisoo Ree and Richmond Sarpong

Reaction scheme
6
Catalytic Enantioselective Addition of Diethyl Phosphite to N-Thiophosphinoyl Ketimines: Preparation of (R)-Diethyl (1-Amino-1-phenylethyl)phosphonate
Shaoquan Lin, Yasunari Otsuka, Liang Yin, Naoya Kumagai, and Masakatsu Shibasaki
Org. Synth. 2017, 94, 313
DOI: 10.15227/orgsyn.094.0313
Checked by: Ayumu Matsuda and Keisuke Suzuki

Reaction scheme
7
Preparation of Sodium Heptadecyl Sulfate (Tergitol-7i)
Brent A. Banasik and Mansour Samadpour
Org. Synth. 2017, 94, 303
DOI: 10.15227/orgsyn.094.0303
Checked by: Felix Pultar and Erick M. Carreira

Reaction scheme
8
Enantioselective Preparation of 5-Oxo-5,6-dihydro-2H-pyran-2-yl phenylacetate via organocatalytic Dynamic Kinetic Asymmetric Transformation (DyKAT)
Tamas Benkovics, Adrian Ortiz, Gregory L. Beutner, and Chris Sfouggatakis
Org. Synth. 2017, 94, 292
DOI: 10.15227/orgsyn.094.0292
Checked by: Simon L. Rössler and Erick M. Carreira

Reaction scheme
9
Rhenium-Catalyzed ortho-Alkylation of Phenols
Yoichiro Kuninobu, Masaki, Yamamoto, Mitsumi Nishi, Tomoyuki Yamamoto, Takashi Matsuki, Masahito Murai, and Kazuhiko Takai
Org. Synth. 2017, 94, 280
DOI: 10.15227/orgsyn.094.0280
Checked by: Austin C. Wright and Brian M. Stoltz

Reaction scheme
10
Preparation of anti-1,3-Amino Alcohol Derivatives Through an Asymmetric Aldol-Tishchenko Reaction of Sulfinimines
Pamela Mackey, Rafael Cano, Vera M. Foley, and Gerard P. McGlacken
Org. Synth. 2017, 94, 259
DOI: 10.15227/orgsyn.094.0259
Checked by: Aymeric Dolbois, Maurus Mathis, Estibaliz Merino, and Cristina Nevado

Reaction scheme
11
Asymmetric Michael Reaction of Aldehydes and Nitroalkenes
Yujiro Hayashi and Shin Ogasawara
Org. Synth. 2017, 94, 252
DOI: 10.15227/orgsyn.094.0252
Checked by: Yasuyuki Ueda and Keisuke Suzuki

Reaction scheme
12
Homologation of Boronic Esters with Lithiated Epoxides
Roly J. Armstrong and Varinder K. Aggarwal
Org. Synth. 2017, 94, 234
DOI: 10.15227/orgsyn.094.0234
Checked by: Philipp Sondermann and Erick M. Carreira

Reaction scheme
13
Preparation of N-Trifluoromethylthiosaccharin: A Shelf-Stable Electrophilic Reagent for Trifluoromethylthiolation
Jiansheng Zhu, Chunhui Xu, Chunfa Xu, and Qilong Shen
Org. Synth. 2017, 94, 217
DOI: 10.15227/orgsyn.094.0217
Checked by: Jon Lorenz and Chris Senanayake

Reaction scheme
14
4-Cyano-2-methoxybenzenesulfonyl Chloride
Elliott D. Bayle, Niall Igoe, and Paul V. Fish
Org. Synth. 2017, 94, 198
DOI: 10.15227/orgsyn.094.0198
Checked by: Kevin Gayler, Aoi Kimishima, and John Wood

Reaction scheme
15
N-Methoxy-N-methylcyanoformamide
Jeremy Nugent and Brett D. Schwartz
Org. Synth. 2017, 94, 184
DOI: 10.15227/orgsyn.094.0184
Checked by: Luke E. Hanna and Sarah Reisman

Reaction scheme
16
Fragment Coupling and Formation of Quaternary Carbons by Visible-Light Photoredox Catalyzed Reaction of tert-Alkyl Hemioxalate Salts and Michael Acceptors
Christopher R. Jamison, Yuriy Slutskyy, and Larry E. Overman
Org. Synth. 2017, 94, 167
DOI: 10.15227/orgsyn.094.0167
Checked by: Anthony Y. Chen, Eric R. Welin, Tyler J. Fulton, and Brian Stoltz

Reaction scheme
17
Buta-2,3-dien-1-ol
Hongwen Luo, Dengke Ma, and Shengming Ma
Org. Synth. 2017, 94, 153
DOI: 10.15227/orgsyn.094.0153
Checked by: Carl A. Busacca and Chris Senanayake

Reaction scheme
18
Dirhodium (II) tetrakis[N-4-bromo-1,8-naphthoyl-(S)-tert-leucinate]
Hélène Lebel*, Henri Piras, and Johan Bartholoméüs
Org. Synth. 2017, 94, 136
DOI: 10.15227/orgsyn.094.0136
Checked by: David Stephens and Richmond Sarpong

Reaction scheme
19
Rhodium(I)-catalyzed Allenic Pauson–Khand Reaction
Joseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond
Org. Synth. 2017, 94, 123
DOI: 10.15227/orgsyn.094.0123
Checked by: Arthur Han and Sarah E. Reisman

Reaction scheme
20
Synthesis of Allenyl Mesylate by a Johnson-Claisen Rearrangement. Preparation of 3-(((tert-butyldiphenyl-silyl)oxy)methyl)penta-3,4-dien-1-yl methanesulfonate
Joseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond
Org. Synth. 2017, 94, 109
DOI: 10.15227/orgsyn.094.0109
Checked by: Susan M. Stevenson and Sarah E. Reisman

Reaction scheme
21
(Z)-Enol p-Tosylate Derived from Methyl Acetoacetate: A Useful Cross-coupling Partner for the Synthesis of Methyl (Z)-3-Phenyl (or Aryl)-2-butenoate
Yuichiro Ashida, Hidefumi Nakatsuji, and Yoo Tanabe
Org. Synth. 2017, 94, 93
DOI: 10.15227/orgsyn.094.0093
Checked by: Yuji Suzuki and Keisuke Suzuki

Reaction scheme
22
Practical Syntheses of [2,2′-bipyridine]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III)hexafluorophosphate, [Ir{dF(CF3)ppy}2(bpy)]PF6 and [4,4′-bis(tert-butyl)-2,2′-bipyridine]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III)hexafluorophosphate, [Ir{dF(CF3)ppy}2(dtbbpy)]PF6
Martins S. Oderinde and Jeffrey W. Johannes
Org. Synth. 2017, 94, 77
DOI: 10.15227/orgsyn.094.0077
Checked by: Nadide Hazal Avcı, Chase Olsson, Brandon Nelson, and Mohammad Movassaghi

Reaction scheme
23
Palladium-catalyzed External-CO-Free Reductive Carbonylation of Bromoarenes
Hideyuki Konishi, Masataka Fukuda, Tsuyoshi Ueda, and Kei Manabe
Org. Synth. 2017, 94, 66
DOI: 10.15227/orgsyn.094.0066
Checked by: Jordan C. Beck and Sarah E. Reisman

Reaction scheme
24
Ugi Multicomponent Reaction
André Boltjes, Haixia Liu, Haiping Liu, and Alexander Dömling
Org. Synth. 2017, 94, 54
DOI: 10.15227/orgsyn.094.0054
Checked by: Emma L. Baker-Tripp and Neil K. Garg

Reaction scheme
25
Site-Selective C-H Fluorination of Pyridines and Diazines with AgF2
Patrick S. Fier and John F. Hartwig
Org. Synth. 2017, 94, 46
DOI: 10.15227/orgsyn.094.0046
Checked by: Matthew G. Beaver, Christopher J. Borths, and Margaret M. Faul

Reaction scheme
26
Continuous Flow Hydration of Pyrazine-2-carbonitrile in a Manganese Dioxide Column Reactor
Claudio Battilocchio, Shing-Hing Lau, Joel M. Hawkins, and Steven V. Ley
Org. Synth. 2017, 94, 34
DOI: 10.15227/orgsyn.094.0034
Checked by: Frederic Buono, Andrew Brusoe and Chris Senanayake

Reaction scheme
27
Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate
Kingson Lin, Christopher B. Kelly, Matthieu Jouffroy, and Gary A. Molander
Org. Synth. 2017, 94, 16
DOI: 10.15227/orgsyn.094.0016
Checked by: Andrés García-Domínguez, Estíbaliz Merino, and Cristina Nevado

Reaction scheme
28
Preparation of Aryl Alkyl Ketenes
Nicholas D. Staudaher, Joseph Lovelace, Michael P. Johnson, and Janis Louie
Org. Synth. 2017, 94, 1
DOI: 10.15227/orgsyn.094.0001
Checked by: Sheng Guo and Dawei Ma

Reaction scheme

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All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors
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