A Publication
of Reliable Methods
for the Preparation
of Organic Compounds
Annual Volume
Volume 98 (2021)
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Mild mono-Acylation of 4,5-Diiodoimidazole: Preparation of 1-(5-Iodo-1H-imidazole-4-yl)pent-4-en-1-one
Michael Morgen, Jasmin Lohbeck, and Aubry K. Miller
Org. Synth. 2021, 98, 171
DOI: 10.15227/orgsyn.098.0171
Checked by: Anji Chen, Hari P. R. Mangunuru, Nathaniel D. Kaetzel, Gopal Sirasani, and Chris Senanayake

Reaction scheme
Synthesis of the Isocyanide Building Block Asmic, anisylsulfanylmethylisocyanide
Embarek Alwedi, Bilal Altundas, Allen Chao, Zachary L. Ziminsky, Maanasa Natrayan, and Fraser F. Fleming
Org. Synth. 2021, 98, 147
DOI: 10.15227/orgsyn.098.0147
Checked by: Anthony J. Fernandes, Martina Drescher, and Nuno Maulide

Reaction scheme
Palladium-Catalyzed Hydrodefluorination of Fluoroarenes
Joseph J. Gair, Ronald L. Grey, Simon Giroux, and Michael A. Brodney
Org. Synth. 2021, 98, 131
DOI: 10.15227/orgsyn.098.0131
Checked by: Vincent Porte, Daniel Kaiser, and Nuno Maulide

Reaction scheme
Discussion Addendum for: Preparation of (S)-tert-ButylPyOx and Palladium-Catalyzed Asymmetric Conjugate Addition of Arylboronic Acids
Stephen R. Sardini and Brian M. Stoltz
Org. Synth. 2021, 98, 117
DOI: 10.15227/orgsyn.098.0117
Original Article: Org. Synth. 2015, 92, 247

Reaction scheme
Synthesis of a Phosphorous Sulfur Incorporating Reagent for the Enantioselective Synthesis of Thiophosphates
Prantik Maity, Amitha S. Anandamurthy, Vijaykumar Shekarappa, Rajappa Vaidyanathan, Bin Zheng, Jason Zhu, Michael A Schmidt, Richard J. Fox, Kyle W. Knouse, Julien C. Vantourout, Phil S. Baran, and Martin D. Eastgate
Org. Synth. 2021, 98, 97
DOI: 10.15227/orgsyn.098.0097
Checked by: Álvaro Gutiérrez-Bonet and Kevin Campos

Reaction scheme
Cu-catalyzed Allylic Perfluoroalkylation of Alkenes Using Perfluoro Acid Anhydrides: Preparation of N-(5,5,5-Trifluoro-2-penten-1-yl)phthalimide
Yuma Aoki, Shintaro Kawamura, and Mikiko Sodeoka
Org. Synth. 2021, 98, 84
DOI: 10.15227/orgsyn.098.0084
Checked by: Martina Drescher, Daniel Kaiser, and Nuno Maulide

Reaction scheme
Palladium-Catalyzed Acetylation of Arylbromides
Milauni M. Mehta, Andrew V. Kelleghan, and Neil K. Garg
Org. Synth. 2021, 98, 68
DOI: 10.15227/orgsyn.098.0068
Checked by: Martina Drescher, Daniel Kaiser, Nuno Maulide, Zach Ariki, Yuki Maekawa, and Cathleen Crudden

Reaction scheme
Reductive Deuteration of Ketones with Magnesium and D2O for the Synthesis of α-Deutero-o-methyl-benzhydrol
Nengbo Zhu, Wen-Ming Wan, and Hongli Bao
Org. Synth. 2021, 98, 51
DOI: 10.15227/orgsyn.098.0051
Checked by: Yuuki Watanabe, Koichi Hagiwara, and Masayuki Inoue

Reaction scheme
Chiral Organoiodine-catalyzed Enantioselective Oxidative Dearomatization of Phenols
Muhammet Uyanik, Shinichi Ishizaki, and Kazuaki Ishihara
Org. Synth. 2021, 98, 28
DOI: 10.15227/orgsyn.098.0028
Checked by: Tao Wang and Kevin Campos

Reaction scheme
Synthesis of Chiral Organoiodine Catalyst for Enantioselective Oxidative Dearomatization Reactions: N,N'-(2S,2'S )-(2-Iodo-1,3-phenylene)bis(oxy)bis(propane-2,1-diyl)bis(2,4,6-trimethylbenzamide)
Muhammet Uyanik, Shinichi Ishizaki and Kazuaki Ishihara
Org. Synth. 2021, 98, 1
DOI: 10.15227/orgsyn.098.0001
Checked by: Cayetana Zarate and Kevin Campos

Reaction scheme

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All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors