A Publication
of Reliable Methods
for the Preparation
of Organic Compounds
Annual Volume
Volume 96 (2019)
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Discussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (R)-(-)-3-Benzyloxy-2-methyl Propanoate
Harvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley
Org. Synth. 2019, 96, 124
DOI: 10.15227/orgsyn.096.0124
Original Article: Org. Synth. 2007, 84, 295

Reaction scheme
Discussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate
Aslam C. Shaikh and Ohyun Kwon
Org. Synth. 2019, 96, 110
DOI: 10.15227/orgsyn.096.0110
Original Article: Org. Synth. 2009, 86, 212

Reaction scheme
Discussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate
Mizzanoor Rahaman and M. Mahmun Hossain
Org. Synth. 2019, 96, 98
DOI: 10.15227/orgsyn.096.0098
Original Article: Org. Synth. 2009, 86, 172

Reaction scheme
Discussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2-(2-acetylphenyl)acetate
Austin C. Wright and Brian M. Stoltz
Org. Synth. 2019, 96, 80
DOI: 10.15227/orgsyn.096.0080
Original Article: Org. Synth. 2009, 86, 161

Reaction scheme
Synthesis of 2,3-Diaryl-2H-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates
Mi-Na Zhao and Zheng-Hui Guan
Org. Synth. 2019, 96, 66
DOI: 10.15227/orgsyn.096.0066

Reaction scheme
Discussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to α,β-Unsaturated Esters: Asymmetric Synthesis of (S)-β:Leucine
Stephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson
Org. Synth. 2019, 96, 53
DOI: 10.15227/orgsyn.096.0053
Original Article: Org. Synth. 2010, 87, 143

Reaction scheme
Nickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate
Yuki Kawashima, Takayuki Furukawa, Naoto Chatani* and Mamoru Tobisu
Org. Synth. 2019, 96, 36
DOI: 10.15227/orgsyn.096.0036
Checked by: Takumi Fukuda, Masanori Nagatomo, and Masayuki Inoue

Reaction scheme
Late-Stage Deoxyfluorination of Phenols with PhenoFluorMix
Junting Chen and Tobias Ritter
Org. Synth. 2019, 96, 16
DOI: 10.15227/orgsyn.096.0016
Checked by: Shota Nagasawa and Richmond Sarpong

Reaction scheme
Discussion Addendum for: 4-Nonylbenzoic Acid
Alois Fürstner
Org. Synth. 2019, 96, 1
DOI: 10.15227/orgsyn.096.0001
Original Article: Org. Synth. 2005, 81, 33

Reaction scheme

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All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors