A Publication
of Reliable Methods
for the Preparation
of Organic Compounds
Annual Volume
Volume 100 (2023)
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Synthesis of a 2,5-Bis(tert-butyldimethylsilyloxy)furan and its Reaction with Benzyne
Jessica E. Budwitz and Christopher G. Newton
Org. Synth. 2023, 100, 159
DOI: 10.15227/orgsyn.100.0159
Checked by: Dave J. Charboneau, Jordan K. Thompson, and Sarah E. Reisman

Reaction scheme
α-Oxamination of Amides via Electrophilic Activation
Miran Lemmerer, Ján Matyašovský, Roberto Tinelli and Nuno Maulide
Org. Synth. 2023, 100, 136
DOI: 10.15227/orgsyn.100.0136
Checked by: Colin Knus, Jaime Martín, Jorge A. González, and Cristina Nevado

Reaction scheme
Kathleen J. Berger, Balu D. Dherange, Megan Morales, Julia L. Driscoll, A. Kaan Tarhan, and Mark D. Levin
Org. Synth. 2023, 100, 113
DOI: 10.15227/orgsyn.100.0113
Checked by: Yinuo Zheng and Pauline Chiu

Reaction scheme
α-Arylation of Cyclopentanones by Palladium/Enamine Cooperative Catalysis
Yibin Xue, Arjuna Parsad, and Guangbin Dong
Org. Synth. 2023, 100, 99
DOI: 10.15227/orgsyn.100.0099
Checked by: Jaejoong Han, Masanori Nagatomo, and Masayuki Inoue

Reaction scheme
Synthesis of Diethyl (1-Diazo-2-oxopropyl)phosphonate
Cholapat Varongchayakul and Rick L. Danheiser
Org. Synth. 2023, 100, 84
DOI: 10.15227/orgsyn.100.0084
Checked by: Michael D. Clift, Steve M. Richter, Zhe Wang, and Seble Wagaw

Reaction scheme
Preparation of N-Boc-3-methylpyrrole via Anionic Rearrangement
Daniel P. Graeff, Noah J. Sims, Quentin R. Savage, Richard K. Jackson, III, Amy C. Jackson, Danielle M. Lawson, Madelyn R. Wixom, and John L. Wood
Org. Synth. 2023, 100, 61
DOI: 10.15227/orgsyn.100.0061
Checked by: Yuya Shiga, Haruka Fujino, and Masayuki Inoue

Reaction scheme
Synthesis of NH-Sulfoximines from Sulfides Using Ammonium Carbamate and (Diacetoxyiodo)benzene to Transfer NH and O
Arianna Tota, Mauro Spennacchio, Edward L. Briggs, Tsz-Kan Ma, Zhenhao Zhong, Leonardo Degennaro, James A. Bull and Renzo Luisi
Org. Synth. 2023, 100, 48
DOI: 10.15227/orgsyn.100.0048
Checked by: Ellie Plachinski and Tehshik Yoon

Reaction scheme
Discussion Addendum for: Rh(I)-Catalyzed Allenic Pauson-Khand Reaction
Eric D. Deihl, Fatemeh Haghighi, and Kay M. Brummond
Org. Synth. 2023, 100, 29
DOI: 10.15227/orgsyn.100.0029
Original Article: Org. Synth. 2017, 94, 123

Reaction scheme
Preparation of Highly-Substituted Pyridines via Diels-Alder Reactions of Vinylallenes and Tosyl Cyanide
Nathan H. Faialaga, Christian Gomez, Samuel G. Bartko, Philipp Natho, and Rick L. Danheiser
Org. Synth. 2023, 100, 4
DOI: 10.15227/orgsyn.100.0004
Checked by: Christopher C. Nawrat and Kevin R. Campos

Reaction scheme
Introducing Volume 100 of Organic Syntheses
Rick L. Danheiser
Org. Synth. 2023, 100, 1
DOI: 10.15227/orgsyn.100.0001

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors