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1
meta-C-H Halogenation of pyridines, quinolines, and isoquinolines: meta-chlorination of 2-phenylpyridine
Pengwei Xu and Armido Studer
Org. Synth. 2024, 101,
524
DOI: 10.15227/orgsyn.101.0524
Checked by: Alexander Sailer and Dirk Trauner
2
Discussion Addendum for: Dipeptide Syntheses via Activated α-Amino Esters
Jean-Marc Campagne and Renata Marcia de Figueiredo
Org. Synth. 2024, 101,
508
DOI: 10.15227/orgsyn.101.0508
3
Hydrodealkenylative Cleavage of C(sp3)-C(sp2) Bonds: Preparation of (1S, 3R)-3-Methylcyclohexan-1-ol
Brady W. Dehnert and Ohyun Kwon
Org. Synth. 2024, 101,
488
DOI: 10.15227/orgsyn.101.0488
Checked by: Matthew Furry, Ryan R. G. Barrett, and Christopher D. Vanderwal
4
Nitrosation of Diphenylamine with 3,3-dimethyl-2-nitroso-2,3-dihydrobenzo[d]isothiazole 1,1-dioxide (NO-1)
Pravien S. Rajaram, Keerthana Chakkanalil, and Ryan D. Baxter
Org. Synth. 2024, 101,
478
DOI: 10.15227/orgsyn.101.0478
Checked by: Haoran Xiong, Hirofumi Ueda, and Hidetoshi Tokuyama
5
Oxygen-free alkene hydration using nitroarenes: Diastereoselective hydration of cholesteryl acetate
Jonas Elfert, Anup Bhunia, and Armido Studer
Org. Synth. 2024, 101,
460
DOI: 10.15227/orgsyn.101.0460
Checked by: Ibrahim-Ethem Celik and Christopher D. Vanderwal
6
Discussion Addendum for: Palladium-catalyzed Buchwald-Hartwig Amination and Suzuki-Miyaura Cross-coupling Reaction of Aryl Mesylates
Yu Kiu Lau, Man Ho Tse, Pui Ying Choy, and Fuk Yee Kwong
Org. Synth. 2024, 101,
438
DOI: 10.15227/orgsyn.101.0438
7
Discussion Addendum for: Preparation of 2-(2-(Dicyclohexylphosphino)phenyl)-1-methyl-1H-indole (CM-phos)
Cheuk Lam Cheung, Pui Ying Choy, Man Ho Tse, and Fuk Yee Kwong
Org. Synth. 2024, 101,
423
DOI: 10.15227/orgsyn.101.0423
8
Synthesis of 3-Azabicyclo[3.2.0]heptane hydrochloride
Carl M. F. Mansson and Noah Z. Burns
Org. Synth. 2024, 101,
410
DOI: 10.15227/orgsyn.101.0410
Checked by: J. Andrew P. Maitland, Daniel J. Cox and Darren J. Dixon
9
Preparation of S-Methyl Methanethiosulfonate from Dimethyl Sulfoxide Initiated by Oxalyl Chloride
Xixuan Zhao, Shuai Peng, Hao Wang, Shuai Huang, Baoguo Sun, Hongyu Tian and Sen Liang
Org. Synth. 2024, 101,
395
DOI: 10.15227/orgsyn.101.0395
Checked by: Roberto Tinelli, Sophie Woolford and Nuno Maulide
10
α-Arylation of N-Boc Pyrrolidine
Kevin Campos, Melissa Cummings, Hengyu Li, and Feng Peng
Org. Synth. 2024, 101,
382
DOI: 10.15227/orgsyn.101.0382
Checked by: Mott and Sarah E. Reisman
11
Synthesis of 3,3-Dimethyl-nitroso-2,3-dihydrobenzo[d]isothiazole 1,1-dioxide (NO-1)
Keerthana Chakkanalil, Pravien S. Rajaram, and Ryan D. Baxter
Org. Synth. 2024, 101,
366
DOI: 10.15227/orgsyn.101.0366
Checked by: Haoran Xiong, Hirofumi Ueda, and Hidetoshi Tokuyama
12
Preparation of Highly Reactive Lithium Metal Dendrites and the Synthesis of (Trimethylsilyl)methyllithium
Raquel M. Gonzalez, Han-Hsiang Hsu, and Andy A. Thomas
Org. Synth. 2024, 101,
342
DOI: 10.15227/orgsyn.101.0342
Checked by: Bilal Altundas and Scott E. Denmark
13
Hydration of Nitriles to Primary Amides Enabled by the Ghaffar-Parkins Catalyst
Daniel W. Turner, Allison T. Hands, and Neil K. Garg
Org. Synth. 2024, 101,
327
DOI: 10.15227/orgsyn.101.0327
Checked by: Kohta Ide, Juri Sakata, and Hidetoshi Tokuyama
14
Synthesis of Benzyl-δ-Truxinate via Enantioselective [2+2] Photocycloaddition
Rodrigo Villanueva, Ellie F. Plachinski, and Tehshik P. Yoon
Org. Synth. 2024, 101,
309
DOI: 10.15227/orgsyn.101.0309
Checked by: Yu-Che Chang and M. Kevin Brown
15
Discussion Addendum for: Palladium-Catalyzed Dehydrative Allylation of Hypophosphorous Acid with Allylic Alcohols. Preparation of Cinnamyl-H-Phosphinic Acid
Karla Bravo-Altamirano and Jean-Luc Montchamp
Org. Synth. 2024, 101,
295
DOI: 10.15227/orgsyn.101.0295
16
Synthesis of S,S-Di(pyridin-2-yl)carbonodithioate (DPDTC) for the Reduction of Carboxylic Acids
Karthik S. Iyer, Jordan R. Yirak, Hubert Muchalski, and Bruce H. Lipshutz
Org. Synth. 2024, 101,
274
DOI: 10.15227/orgsyn.101.0274
Checked by: Anna A. M. Miller, Daniel Rozsar and Darren J. Dixon
17
One-pot Synthesis of Alkynes from Esters via a Tandem Reduction-Ohira-Bestmann Reaction
Cholapat Varongchayakul and Rick L. Danheiser
Org. Synth. 2024, 101,
258
DOI: 10.15227/orgsyn.101.0258
Checked by: Hojoon Park and Kevin R. Campos
18
Preparation of 2-Chloro-1-(1-ethoxyvinyl)pyridinium Triflate
John P. Frank, William R. Strutton, Joel K. A. Adade, and Max M. Majireck
Org. Synth. 2024, 101,
242
DOI: 10.15227/orgsyn.101.0242
Checked by: Christopher C. Nawrat and Kevin Campos
19
Platinum-Catalyzed Enantioselective Diboration of Monosubstituted Alkenes
Chenpeng Gao, Paul S. Lee, and James P. Morken
Org. Synth. 2024, 101,
229
DOI: 10.15227/orgsyn.101.0229
Checked by: Matthieu Maciejewski and Tehshik Yoon
20
Chromatography-Free and Chlorinated Solvent-Free Preparation of 2,5-dibromohexanediamide (DBHDA)
Ben Bower, Sébastien R. G. Galan, and Benjamin G. Davis
Org. Synth. 2024, 101,
207
DOI: 10.15227/orgsyn.101.0207
Checked by: Ruby Long Ying Chan and Pauline Chiu
21
Intramolecular Coupling for General Synthesis of Backbone Substituted Bicyclo[1.1.1]pentyl Boronates
Jet Tsien, Yangyang Yang, René García-Del Valle, Jonathan M. E. Hughes, Byron K. Peters, Rohan R. Merchant, and Tian Qin
Org. Synth. 2024, 101,
181
DOI: 10.15227/orgsyn.101.0181
Checked by: Sota Akiyama, Paul Sinclair and Richmond Sarpong
22
Difluoromethylation of Phenols
Allison T. Hands, Zachary G. Walters, Jacob P. Sorrentino, and Neil K. Garg
Org. Synth. 2024, 101,
164
DOI: 10.15227/orgsyn.101.0164
Checked by: Yi Xiao, Milos Vavrik and Nuno Maulide
23
Nickel-catalyzed Amination of Aryl Chlorides
Zachary G. Walters, Daniel W. Turner, and Neil K. Garg
Org. Synth. 2024, 101,
150
DOI: 10.15227/orgsyn.101.0150
Checked by: Prashansa B. Kannangara and M. Kevin Brown
24
Tandem Fragmentation/Olefination for Production of Neopentylene-Tethered 1,6-Enynes from Dimedone
Kh Tanvir Ahmed, A. C. Martin, Gabriella O. Wabler, Kristen S. Nerbecki, and Gregory B. Dudley
Org. Synth. 2024, 101,
124
DOI: 10.15227/orgsyn.101.0124
Checked by: Hyung Joo Kim and Tehshik Yoon
25
Synthesis of 5-(1-Diazo-2-ethoxy-2-oxoethyl) dibenzo[b,d]thiophenium Triflate
Brigitte Worbs, Sven Timmann, Feng Peng, Ralph Zhao, and Manuel Alcarazo
Org. Synth. 2024, 101,
109
DOI: 10.15227/orgsyn.101.0109
Checked by: Partha Sarathi Hazra and Kevin Brown
26
Discussion Addendum for: Mild Conversion of Tertiary Amides to Aldehydes Using Cp2Zr(H)Cl (Schwartz's Reagent)
Narsihmulu Cheryala, Rui Shi, Shelby Mcguire, Naresh Gantasala, Nagarjun Reddy Vantaddu, Ravikrishna Dada, Nan Wang, Shameem S. Syeda, Hira Khalid, and Gunda I. Georg
Org. Synth. 2024, 101,
81
DOI: 10.15227/orgsyn.101.0081
27
Preparation of Radical Clocks Bearing Carbonyl Groups: Synthesis of N-Methoxy-N-methylspiro[cyclopropane-1,9'-fluorene]-2-carboxamide
Nicole D. Bartolo, Ryan N. Robson, Collin H. Witt, and K. A. Woerpel
Org. Synth. 2024, 101,
61
DOI: 10.15227/orgsyn.101.0061
Checked by: Kevin Lee and Dirk Trauner
28
Cobalt-catalyzed Radical Olefin Isomerization: Retrocycloisomerization of (-)-Caryophyllene Oxide to (-)-Humulene Oxide II
Eleanor M. Landwehr and Ryan A. Shenvi
Org. Synth. 2024, 101,
51
DOI: 10.15227/orgsyn.101.0051
Checked by: Emily P. Chen and Sarah E. Reisman
29
Metal-Free Aziridination of Alkenes with Free Amines by Thianthrenation
Ming-Shang Liu and Wei Shu
Org. Synth. 2024, 101,
34
DOI: 10.15227/orgsyn.101.0034
Checked by: Michael D. Zott and Dirk Trauner
30
Synthesis of Deuterated 1H-Indole-3-carboxaldehyde via Catalytic Vilsmeier-Haack Reaction
Jing Xue, Yushan Zhang, Bing Zhong and Jin-Dong Yang
Org. Synth. 2024, 101,
21
DOI: 10.15227/orgsyn.101.0021
Checked by: Paolo Piacentini, Omar Abdo and Nuno Maulide
31
Synthesis of Secondary Benzylic Alcohols by Reductive Arylation of Aldehydes: α-Phenyl-6-quinolinemethanol
Gilian T. Thomas, Eric S. Isbrandt and Stephen G. Newman
Org. Synth. 2024, 101,
1
DOI: 10.15227/orgsyn.101.0001
Checked by: Christopher C. Nawrat and Kevin Campos
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